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DIOXIN96
16th Symposium on Chlorinated Dioxins and Related CompoundsAmsterdam, August 12-16, 1996
Organohalogen Compounds, Volume 28Short Papers
Editors: Kees Olie
Robert Louw
Jacob de Boer
Erik Evers
Heidelore Fiedler
Jan Hendriks
Ronald Hites
Narayanan Kannan
Djien Liem
Ross Norstrom
Michael Oehme
Mats Tysklind
Job van Zorge
UNIVERSITATSBI3LIOTHEKHANNOVER
TECHNISCHEiNFORMATIONSBIBLIOTHEK
UB/TIB Hannover115 350 586
89
Transport & FateEnvironmental LevelsToxaphenes, PCB's and other Non-Dioxins
TABLE OF CONTENTSVolume 28
Transport & Fate (FATE)
FATE ITransport & Fate
Wendy A. Lead, Jones K.C. (United Kingdom)The cold condensation & global fractionation hypotheses: The search forsupporting evidence 1
Harrie A.J. Govers, Krop H.B. (The Netherlands)Partition constants of chlorinated dibenzofurans and dibenzo-p-dioxins 5
Shin-ichi Sakai, Urano S., Takatsuki H., Shiozaki K., Gokita K. (Japan)Influences of humic acid and linear alkylbenzen sulfonate (LAS) on leachingbehavior of PCDDs/PCDFs from shredder residues 11
Noriyuki Suzuki, Yasuda M., Sakurai T., Nakanishi J. (Japan)M o d e l i n g t he p r o f i l e t r a n s f o r m a t i o n o f P C D D s a n d PCDFs in t h e e n v i r o n m e n t . . . 16
Michel Lebeuf, Gobeil C , Brochu C , Moore S. (Canada)Direct atmospheric deposition versus fluvial inputs of PCDD/Fs to thesediments of the Lower St. Lawrence Estuary 20
John Sandal Is, Berryman B., Bennett L, Newstead S., Fox A. (United Kingdom)Dioxins on land around a chemicals waste incinerator and assignment of source . . 25
Jianwen She, Hagenmaier H. (U.S.A.)Levels and rate of PCDD/Fs soil around Rastatt in Southwest Germany 31
Svetozar Polic, Leskovsek H. (Slovenia)Fate and transport of polychlorinated biphenyls (PCBs) between water andatmosphere of the polluted Krupa River in Slovenia 35
FATE IIFate Degradation
John Parsons, De Bruijne J.A., Goorissen H., Weiland A.R. (The Netherlands)Biogradation of chilorinated dioxins and dibenzofurans by thebiphenyl-utilizing strain JB1 39
Merel Toussaint, Van der Steen J., Parsons J.R., De Wolf J.,Beurkens J.E.M. (The Netherlands)Reductive dechlorination of chlorinated dibenzo-p-dioxins by abacterial consortium isolated from Lake Ketelmeer sediment 44
table of contents, p. 1
FATE (po)Transport & Fate (posters)
Patrik L. Andersson, Hagland P., Tysklind M. (Sweden)Rotational barrier of the polychlorinated biphenyls as a physico-chemicalparameter for use in modelling of QSARs and QSPRs 47
Claudia Bock, Harms H. (Germany)Metabolism of selected polychlorobiphenyl congeners in plant cell cultures 53
Ian T. Cousins, Hartlieb N., Teichmann C , Jones K.C. (United Kingdom)Volatilisations of polychlorinated biphensyls from sludge-amended soils 58
Satoshi Takada, Matsueda T., Kondo R., Sakai K. (Japan)Metabolites of 2,3,7,8-tetrachloro-and octachloro-dibenzo-p-dioxin, anddegradation of PCDDs and PCDFs in a fly ash sample by the White Rot FungusPhanerochaete sordida YK-624 64
Mats Tysklind, Andersson P.L., Strandberg B., Wagman N. (Sweden)Selection of PCBs for laboratory testing or use as indicators inenvironmental monitoring 68
Kerstin Welsch-Pausch, McLachlan M.S. (Germany)Pathways of atmospheric PCDD/F in a native grassland culture:The importance of particle-bound deposition 72
table of contents, p. 2
Environmental Levels
ENVI IEnvironmental Levels (General)
David H. Cleverly, Monetti M., Phillips L., Cramer P., Heit M., McCarthy S.,O'Rourke K., Stanley J., Winters D. (U.S.A.)A time-trend study of the occurrences and levels of CDDs, CDFs anddioxin-like PCBs in sediment cores from 11 geographically distributed lakesin the United States 77
Christoph Lau, Fiedler H., Hutzinger O., Rippen G., Wesp H.F., Sievers S.,Friesel P., Schacht U., Gras B., Reich T., Vahrenholt F. (Germany)Dioxin mass balance for the city of Hamburg, Germany. Part 1:Objective of the study and emission inventory 83
Peter Friesel, Sievers S., Fiedler H., Gras B., Lau C, Reich T.,Rippen G., Schacht U., Vahrenholt F. (Germany)Dioxin mass balance for the city of Hamburg, Germany. Part 4: Follow upstudy - trends of PCDD/PCDF fluxes 89
Thomas Webster, Connett P. (U.S.A.)Dioxin emission inventories: The importance of large sources 95
Hanspaul Hagenmaier, Walczok M. (Germany)Time trends in levels, patterns and profiles for PCDD/PCDF in sedimentcores of Lake Constance 101
Chris Rappe, Andersson R., Bonner M.S., Cooper K.R., Fiedler H.,Howell F.G., Lau C. (Sweden)PCDDs and PCDFs in municipal sewage sludge and effluent from theState of Mississippi, USA 105
Dennis J. Paustenbach, Wenning R.J., Mathur D., Luksemburg W. (U.S.A.)PCDDs and PCDFs in Urban Stormwater Discharged to San Francisco Bay,California USA 111
Erik H.G. Evers, Laane R.W.P.M., Groeneveld G.J.J., Olie K.(The Netherlands)Levels, temporal trends and risk of dioxins and related compounds inthe Dutch aquatic environment 117
ENVI IIEnvironmental Levels (Air)
Joseph Ferrario, Byrne C , Dupuy Jr. A.E. (U.S.A.)Coplanar polychorinated biphenyl (PCB) background contaminationin trace level analytical procedures 123
table of contents, p. 3
Karen B. Riggs, Roth A., Kelly T.J., Schrock M.E. (U.S.A.)Ambient PCDD/PCDF levels in Montgomery County, Ohio: Comparison toprevious data and source attribution 128
Maximilian Swerev, Nordsieck H., Pawlik V., Hutzinger O. (Germany)Impact of emissions of modern waste incinerators on atmosphericconcentrations of PCDD and PCDF 134
Simon J. Buckland, Howard K.E., Salter R.T. (New Zealand)Assessment of the New Zealand environment for the levels ofPCDDs, PCDFs, PCBs and other organochlorine contaminants 140
Matthew Lorber, Braverman C , Gehring P., Winters D.,Sovocool W. (U.S.A.)Soil and air monitoring in the vicinity of a municipal solidwaste incinerator. Part II: Air monitoring 146
ENVI IIIEnvironmental Levels (Food)
Vernon J. Feil, Davison K.L., Tierman T.O., Anderson V.L. (U.S.A.)Distribution of polychlorinated dioxins and furans in beef 152
George F. Fries, Feil V.J., Davison K.L. (U.S.A.)The significance of pentachlorophenol-treated wood as a source ofdioxin residues in United States beef 156
Andrew A. Lovett, Foxall CD. , Creaser C.S., Chewe D. (United Kingdom)PCB and PCDD/DF concentrations in egg and poultry meat samplesfrom urban and rural areas in Wales and England 160
Arnold Schecter, Papke O., Dellarco M., Olson J. (U.S.A.)A c o m p a r i s o n o f d i o x i n s a n d d i b e n z o f u r a n s i n c o o k e d a n d u n c o o k e d f o o d . . . . 1 6 6
Rustem Z. Khamitov, Simonova N., Maksimov G., Maystrenko V.N. (Russia)Chlorinated dioxin and dibenzofuran levels in food from BashkortostanRepublic, Russia 171
ENVI (po)Environmental Levels (posters)
Abad E., Caixach J., Rivera J. (Spain)Analisys of PCDD/PCDF from emissions sources and ambient air inNortheast of Spain 1 75
Osomu Aozasa, Ikeda M., Nakao T., Ohta S., Miyata H., Huang C.-W.,Tsai H. (Japan)Air pollution by PCDDs, PCDFs and non-ortho coplanar PCBs in Japanusing pine needle as a biomonitoring indicator 181
table of contents, D. 4
Samuel Atuma, Linder C.-E., Bergh A., Wicklund-Glynn A., Andersson 6.,Johnsson H. (Sweden)Levels of selected coplanar PCBs in fish from the Swedish waterenvironment 187
Peter Behnisch, Engelhart A., Apfelbach R., Hagenmaier H. (Germany)Occurence of non-ortho, mono-ortho and di-ortho substituted PCBcongeners in polecats, stone martens and badgers from the state ofBaden-Wurttemberg, Germany 191
Keith R. Cooper, Bergek S., Fiedler H., Hjelt M., Bonner M.S.,Howell F.G., Rappe C. (U.S.A.)PCDDs, PCDFs and PCBs in farm raised catfish from southeastUnited States 197
Eckhard Denker, Alawi M.A., Buthe A. (Germany)PCB pattern in two fish species from the Gulf of Akaba, Jordan 203
Daniel Fraisse, Schnepp B., Mort-Bontemps C, Le Querrec F. (France)Levels of polychlorodibenzo-dioxins (PCDDs) andpolychlorodibenzo-furans (PCDFs) in milk in France 209
William Gillespie, Abbott J.D. (U.S.A.)Progess in reducing the TCDD/TCDF content of releases from bleachedpulp mills and fish taken below mill discharges 213
Jon Knutzen, Schlabach M. (Norway)Summary of data on toxicity equivalents from PCDF/PCDD and non-orthoPCB in marine organisms and sediments from Norway 219
Jutta Kohler, Peichl L. (Germany)Monitoring of PCDD/F with Kale 224
Edward A. Kruglov, Amirova Z.K., Loshkina E.A. (Russia)PCDDs and PCDFs in snow coat of an industrial city and as a result ofoil incineration at accident place 228
Yoichi Kurokawa, Matsueda T., Matayoshi N., Satoshi T., Kazumi F. (Japan)Distribution of polychlorinated dibenzo-p-dioxins and dibenzofurans invarious sizes of airborne particles 232
Christoph Lau, Fiedler H., Hutzinger O., Rippen G., Wesp H.F.,Sievers S., Schacht U., Friesel P., Gras B., Vahrenholt F. (Germany)Dioxin mass balance for the city of Hamburg, Germany. Part 2:Flux of PCDD/PCDF with liquid and solid wastes 237
Michel Lebeuf, Moore S., Brochu C. (Canada)The influence of PCBs and PCDFs in the sediments of Baie des Anglaison the Lower St.Lawrence Estuary 243
table of contents, p. 5
Yvonne M. Liske, Kapila S., Spreng A.C., Schreiber R.J. (U.S.A.)An assessment of polychlorinated dibenzo-p-dioxins and furans in rawmaterials for cement production 249
Matthew Lorber, Braverman C, Gehring P., Winters D., Sovocool W. (U.S.A.)Soil and air monitoring in the vicinity of a municipal solid wasteincinerator. Part I: Soil monitoring 255
William J. Luksemburg, Mitzel R.S., Zhou H., Hedin J.H., Silverbush B.B.,Wong A.S. (U.S.A.)Polychlorinated dioxins and dibenzofurans in environmental samplesfrom China 262
Janina Lulek (Poland)Determination of polychlorinated biphenyls in waste motor andtransformer oils 267
Rainer Malisch (Germany)Dioxin-like PCB in food and breast milk samples 271
Rainer Malisch (Germany)PCDD/PCDF-intake from food in the South-Western part of Germany 277
Rainer Malisch, Saad M.M. (Germany)PCDD/PCDF in butter samples from Egypt 281
Wolfgang Moche, Thanner G. (Austria)Ambient air concentrations of dioxins in Austrian conurbations 286
Wolfgang Moche, Thanner G. (Austria)Ambient air concentrations of dioxins during stable weather conditions 291
Anders Olsson, Bergman A., Vitinsh M. (Sweden)Relative concentrations of PCB congeners in perch (Perca fluviatilis) asan indicator of fresh input of PCB near the Daugava river mouth in Latvia 295
Peter Rabl, Dumler-Gradl R., Thoma H., Vierle O. (Germany)PCDD/F-lmmission measurements in different distances from a emissionsource 300
Lourdes Ramos, Eljarrat E., Hernandez L.M., Alonso L., Rivera J.,Gonzalez M.J. (Spain)Levels of PCDDs and PCDFs in farm cow's milk located near potentialcontaminant sources in Asturias (Spain). Comparison with levels foundin control points and commercial pasteurized cow's milks 304
table of contents, p. 6
Fabrizio Rodriguez, Carere C, Dell'Omo G., lacovella N.,Baldassarri L.T., Volpi F., Di Domenico A. (Italy)The Common Swift: A synanthropic bird species for monitoring airbornemicrocontaminants? 308
Takeo Sakurai, Suzuki N., Masunaga S., Nakanishi J. (Japan)Application of principal component analysis to isomer-specific datamatrix of PCDDs and PCDFs 314
Arnold Schecter, Cramer P., Boggess K., Stanley J., Olson J.R.,Kessler H. (U.S.A.)Dioxin intake from U.S. food: Results from a new nationwide food survey 320
Martin Schlabach, Biseth A., Gundersen H. (Norway)Sampling and measurement of PCDD/PCDF and non-ortho PCB in arcticair at Ny-Alesund, Spitsbergen 325
Marta Schuhmacher, Granero S., Domingo J.L., Rivera J., Eljarrat E. (Spain)Levels of PCDD/F in soil samples in the vicinity of a municipal solidwaste incinerator 330
Der-Kau Soong, Ling Y.-C. (Taiwan, ROC)Dioxin in soil samples at a chlorophenal manufacturing site in Taiwan 335
Terttu Vartiainen, Mannio J., Strandman T. (Finland)Concentrations of PCDDs, PCDFs and coplanar PCBs in fish fromsubarctic lakes in Finland 340
Monica Waber, Kohler J., Peichl L. (Germany)Polychlorinated biphenyl (PCB) contents in Curly Kale cultures inthe conurbation of Munich, Germany 344
Dwain Winters, Cleverly D., Lorber M., Meier K., Dupuy A., Byrne C ,Deyrup C , Ellis R., Ferrario J., Leese W., Schaum J., Walcott J.(U.S.A.)Coplanar polychlorinated biphenyls (PCBs) in a national sample of beefin the United States: preliminary results 350
table of contents, p. 7
Toxaphenes (TOXA)
TOXA IToxaphenes
Vladimir A. Nikiforov, Tribulovich V.G., Bolshakov S. (Russia)Structure-behaviour relationships for toxaphene congeners. I.Gas chromatography of chlorinated bomanes 355
Walter Vetter, Miiller U., Krock B., Luckas B. (Germany)Structures and GC retention times of persistent compounds oftechnical toxaphene (CTTs) 359
Jacob de Boer, De Geus H.-J., Brinkman U.A.Th. (The Netherlands)Multidimensional gas chromatographic analysis of toxaphene - testof different column combinations 363
Heidi Karlsson, Oehme M. (Switzerland)Comparison of retention time overlaps of toxaphene congeners on threedifferent stationary phases in cod liver samples and consequences forquantification 369
Mehmet Coelhan, Parlar H., Angerhofer D., Kimmel L. (Germany)A contribution to the HRGC-MS and HRGC-ECD determination of taxopheneresidues in fish 375
Gary A. Stern, Muir D.C.G., Billick B., Lockhart L., Wilkinson P.,Miskimmin B.M. (Canada)Toxaphene congener patterns in lake sediment 379
Vyacheslav G. Tribulovich, Nikiforov V.A., Bolshakov S. (Russia)Isolation and structure elucidation of polychlorodihydrocamphenes- potential constituents of toxaphene residues 385
Susan T. Glassmeyer, Myers T.R., De Vault D.S., Hites R.A. (U.S.A.)Taxophene in Great Lakes fish: A temporal, spatial and trophic study 389
TOXA IIToxaphenes
Deborah L. Swackhamer, Pearson R.F., Schottler S. (U.S.A.)A mass balance of taxophene in the Great Lakes of North America 395
Terry L. Wade, Chambers L., Gardinali P.R., Sericano J.L.,Jackson T.J., Allen-Gill S.M. (U.S.A.)Toxaphene analyses of fish livers by high resolution mass spectrometry 399
table of contents, p. 8
Heidi Karlsson, Oehme M., Muller L. (Switzerland)Enantioselective separation of toxaphene congeners. Results,problems and challenges 405
Lutz Alder, Palavinskas R., Andrews P. (Germany)Enantioselective determination of toxaphene components in fish,monkey adipose tissue from a feeding study and human milk 410
Jan P. Boon, Helle M., Dekker M., Sleiderink H.M., Klamer H.J.,Govers B., Wester P., De Boer J., De Leeuw J.W. (The Netherlands)In-vitro biotransformation of chlorinated bornanes (toxaphene) inhepatic microsomes of marine mammals and birds. Influence onbioaccumulation and mutagenicity 416
Mahmoud A. Saleh (U.S.A.)Recent knowledge on the toxicological properties of toxaphene 422
TOXA (po)Toxaphenes and Other Non-Dioxins (posters)
Lutz Alder, Palavinskas R., Nikiforov V.A., Tribulovich V.G. (Germany)Relative response factors for toxaphene components using different detectors . . . 423
Lutz Alder, Karl H. (Germany)Determination of toxaphene (Camphechlor) residues in foodstuff 429
Kai Bester, Ellerichmann T., Hiihnerfuss H., Moller K., Rimkus G.,Wolf M. (Germany)On the presence of hepta- and hexachlorostyrenes in addition tooctachlorostyrene in fish samples from the river Elbe 433
Bianca Bethan, Bester K., Hiihnerfuss H., Rimkus G. (Germany)Contamination and gas chromatographic chiral separation of bromocyclenin water and fish samples from the river Stor in the northern part ofGermany and in some sewage plant's waste water 437
Rosa Dumler-Gradl, Langhojer J., Miekisch W., Tartler D., Thoma H.,Vierle O. (Germany)Solvolysis of flame retarded circuit boards 441
Jerzy Falandysz, Strandberg L., Bergqvist P.-A., Strandberg B.,Rappe C. (Sweden)Chloronaphthalenes in stickleback Gasterosteus aculeatus from thesouthwestern part of the Gulf of Gdansk, Baltic Sea 446
Jerzy Falandysz, Strandberg L., Strandberg B., Bergqvist P.-A.,Rappe C. (Sweden)Spatial distribution of chlordane compounds in plankton from thesouthern part of the Baltic Sea 452
table of contents, p. 9
Lev A. Fedorov, Dostovalova V.I. (Russia)The prediction of NMR 13C chemical shifts for mixed Cl,Br-benzenesin frame of two-particel increments 456
Rauf V. Galiulin, Galiulina R.R., Bashkin V.N. (Russia)Predecessors of dioxins - DDT and PCBs in irrigated agrolandscapes ofRussia and Uzbekistan 459
Eva Jakobsson, Hu J., Marsh G., Eriksson L. (Sweden)Synthesis and characterization of twenty-eight brominated diphenyl ethers 463
Roland Kallenborn, Haugen J.-E., Nybe S. (Norway)Taxophenes and other organochlorines in dippers {Cinclus cinclus L.)from Southern Norway 469
Bernd Krock, Vetter W., Luckas B. (Germany)PCB - toxaphene group seperation on silica for interference freequantitation of toxaphene residues in environmental samples by GC/ECD 473
Lidia Strandberg, Falandysz J., Strandberg B., Bergqvist P.-A., Rappe C ,Kawano M., Tanaka Y. (Poland)Biomagnification of chlordane compounds by harbour porpoisePhocoena phocoena 478
Don T. Waite, Gurprasad N.P., Constable M.B. (Canada)Concentrations of pentachlorophenol and some related compounds inseasonally collected atmospheric samples from five Canadian locations 482
Kensei Yasuda, Shinoda K., Nakajima T. (Japan)Transchlorination between chlorinated benzenes and benzeneinto chlorobenzene 487
PCB'sMetabolites / Toxicity
Gerald Larsen, Feil V.J., Hakk H., Huwe J.K., Petroske E. (U.S.A.)Polychlorodibenzo-p-dioxin metabolism 491
Eva Klasson-Wehler, Jakobsson E., Orn U. (Sweden)Metabolism of polychlorinated naphthalenes and a tetrabrominateddiphenyl ether 495
Robert J. Letcher, Norstrom R.J., Muir D.C.G. (Canada)The bioaccumulation and metabolic formation of methyl sulfone PCBand 4.4'-DDE metabolites in the polar bear food chain 500
table of contents, p. 10
Johan Lund, Andersson O., Barnes H.J., Gillner M., Hultenby K.,Hard T., Larsson C, Nord M., Nordlund-Moller L., Stripp B. (Norway)Structure and function of a clara cell secretory protein: A determinantof methylsulfonyl-PCB bioaccumulation 506
A. Gerlienke Schuur, Van Meeteren M.E., Jong W.M.C., Brouwer A.,Visser Th.J., Bergman A. (The Netherlands)Inhibition of thyroid hormone sulfation by hydroxylated metabolites ofpolychlorinated biphenyls in vitro 509
Yoshihisa Kato, Haraguchi K., Tomiyasu K., Saito H., Masuda Y.,Kimura R. (Japan)Evidence that 3-methylsulfonyl metabolite of 2,2',4,5,5'-pentachlorobiphenylis causative substance of induction of hepatic microsomal drug-metabolizingenzymes by the parent compound of rats 513
Pirn de Voogt, Van Raat P., Rozemeijer M., Green N. (The Netherlands)Methyl sulfonyl PCBs in cormorant chicks from the Netherlands 517
Cecilia Weistrand, Noren K., Grimelius L. (Sweden)Methyl sulphone metabolites of PCB and DDE in human adipose tissue and liver 522
NON-DIOX IBrominated Polyaromatic Compounds
Ulla Sellstrdm, Kierkegaard A., De Wit C, Jansson B., Asplund L.,Bergander L., Bignert A., Odsjo T., Olsson M. (Sweden)Polybrominated diphenyl ethers (PBDE) in the Swedish environment -a summary 526
Thomas Wanke, Vehlow J., Mark F.E., Brenner K.S. (Germany)The influence of flame retarded plastic foams upon the formation ofBr containing dibenzo-p-dioxins and dibenzofurans in a MSWI 530
NON-DIOX IIOther Halogenated Aromatic Coumpounds
Barbara R. Hillery, Hites R.A. (U.S.A.)Temporal trends in a long term study of vapor phase PCB concentrationsover the Great Lakes 536
Gary A. Stern, Tomy G.T., Muir D.C.G., Westmore J.B., Fisk A.T.,Cymblisty Ch.D. (Canada)Quantifying chlorinated n-alkanes in environmental samples by highresolution gas chromatography electron capture negative ion high resolutionmass spectrometry 540
table of contents, p. 11
Mats Tysklind, Elg K., Andersson P.L., Van Bavel B., Haglund P. (Sweden)The use of multivariate experimental design in the selection ofpolychlorinated naphthalenes for screening of biochemical andtoxicological effects 545
Ruth L. Stringer, Jacobs M.N., Johnston P.A., Wyatt C.L., Santillo D.(United Kingdom)Organochlorine residues in fish oil dietary supplements 551
table of contents, p. 12
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